ECTSElectrochemical Methods: Fundamentals and Applications

Electrochemical Methods: Fundamentals and Applications (CEAC554) Course Detail

Course Name Course Code Season Lecture Hours Application Hours Lab Hours Credit ECTS
Electrochemical Methods: Fundamentals and Applications CEAC554 Elective Courses 3 0 0 3 5
Pre-requisite Course(s)
CEAC 104
Course Language English
Course Type Technical Elective Courses
Course Level Natural & Applied Sciences Master's Degree
Mode of Delivery Face To Face
Learning and Teaching Strategies Lecture, Discussion, Question and Answer.
Course Coordinator
Course Lecturer(s)
  • Prof. Dr. Atilla Cihaner
Course Assistants
Course Objectives The aim of the course explains electrochemical methods and fundamentals and gives an overview of application areas. It explains electrochemical methods like Potentiometry, coulometry, voltammetry, chronometry, polarography etc. Also, the course explains how electrochemical methods can be used with other spectroscopic (UV-vis, ESR, impedance). It explain the preparation and cleaning of the electrodes which are used in electrochemical studies.
Course Learning Outcomes The students who succeeded in this course;
  • Discuss an overview of terminology, fundamental equations, and electrochemical concepts.
  • Describe experimental electrochemical methods.
  • Explain basic equilibrium measurements and Nernst equation.
  • Explain potentiometry, coulometry, chronometry, and polarography methods.
  • Explain how the electrodes can be prepared and cleaned.
  • Explain how the electrochemistry can be used with other spectroscopic methods.
  • Describe common methods like UV-vis, ESR ve impedance.
Course Content General electrochemical concepts, electroanalysis, introduction to electrochemistry, equilibrium measurements, potentiometry, voltammetry, coulometry, chronometry, polarography, rotating electrodes, rate constants of electron transfer, spectroelectrochemistry, electrochemical ESR spectrometry, impedance, electrode preparation methods, cleaning

Weekly Subjects and Releated Preparation Studies

Week Subjects Preparation
1 Electroanalysis, Nomenclature, and Terminology 1-10
2 An Overview of Experimental Methods 11-24
3 Equilibrium Measurements 25-44
4 Equilibrium Measurements 44-84
5 Potentiometry 85-96, 96-106
6 MID-TERM 1
7 Coulometry 107-130
8 Chronometry and Polarogrophy 136-155
9 Rotating Electrode, Rate Constants of Electron Transfer 195-236
10 Spectroelectrochemistry 239-247
11 Electrochemical ESR Spectroscopy 147-153
12 İmpedans 253-270, 270-274
13 MID-TERM 2
14 Electrode Preparation: Cleaning Electrode Surfaces 276-280
15 Elektrot Hazırlama: Elektrot Yapımı, Referans Elektrot Yapımı, Miktoelektrotlar 280-286, 286-288
16 FINAL

Sources

Course Book 1. P. Monk, Fundamentals of Electroanalytical Chemistry, John Wiley & Sons LTD, 2001.
Other Sources 2. Christopher M. A. Brett, Ana Maria Oliveira Brett, Electrochemistry Principles, Methods, and Applications, 2nd Edition, Oxford University Press Inc., 1993.
3. Waldfried Plieth, Electrochemistry for Materials Science, 1nci Baskı, Elsevier Inc., 2008.
4. Cynthia G. Zoski, Handbook of Electrochemistry, 1nci Baskı, Elsevier Inc., 2007.
5. Frano Barbir, PEM Fuel Cells: Theory and Practice, 1nci Baskı, Elsevier Inc., 2005.
6. Allen J. Bard, Larry R. Faulkner, Electrochemical Methods: Fundamentals and Applications, 2nci Baskı, John Wiley & Sons, Inc.,2001.

Evaluation System

Requirements Number Percentage of Grade
Attendance/Participation - -
Laboratory - -
Application - -
Field Work - -
Special Course Internship - -
Quizzes/Studio Critics - -
Homework Assignments - -
Presentation - -
Project - -
Report - -
Seminar - -
Midterms Exams/Midterms Jury 2 60
Final Exam/Final Jury 1 40
Toplam 3 100
Percentage of Semester Work 60
Percentage of Final Work 40
Total 100

Course Category

Core Courses
Major Area Courses X
Supportive Courses
Media and Managment Skills Courses
Transferable Skill Courses

The Relation Between Course Learning Competencies and Program Qualifications

# Program Qualifications / Competencies Level of Contribution
1 2 3 4 5
1 An ability to access, analyze and evaluate the knowledge needed for the solution of advanced chemical engineering and applied chemistry problems. X
2 An ability to self-renewal by following scientific and technological developments within the philosophy of lifelong learning. X
3 An understanding of social, environmental, and the global impacts of the practices and innovations brought by chemistry and chemical engineering. X
4 An ability to perform original research and development activities and to convert the achieved results to publications, patents and technology. X
5 An ability to apply advanced mathematics, science and engineering knowledge to advanced engineering problems. X
6 An ability to design and conduct scientific and technological experiments in lab- and pilot-scale, and to analyze and interpret their results. X
7 Skills in design of a system, part of a system or a process with desired properties and to implement industry. X
8 Ability to perform independent research. X
9 Ability to work in a multi-disciplinary environment and to work as a part of a team. X
10 An understanding of the professional and occupational responsibilities. X

ECTS/Workload Table

Activities Number Duration (Hours) Total Workload
Course Hours (Including Exam Week: 16 x Total Hours) 16 3 48
Laboratory
Application
Special Course Internship
Field Work
Study Hours Out of Class 16 1 16
Presentation/Seminar Prepration
Project
Report
Homework Assignments
Quizzes/Studio Critics
Prepration of Midterm Exams/Midterm Jury 2 20 40
Prepration of Final Exams/Final Jury 1 21 21
Total Workload 125